tert-Butyl hydroperoxide (40 ml of a 5M solution in decanes, 200 mmol, 2 eq.) was added via cannula to a solution of (2E)-oct-2-en-1-ol 23 (MW=128.21, d=0.850, 12.8 g, 15.1 ml, 100 mmol) in DCM (200 ml)
XML version
<reaction id="r12312"
xmlns:nist="http://units.nist.gov"
xmlns:iupac="http://www.iupac.org/solvents"
xmlns:rsc="http://www.rsc.org/reagents"
xmlns="http://www.xml-cml.org">
<substance role="reagent" ref="rsc:a213123"
title="tert-Butyl hydroperoxide">
<amount units="nist:ml">40</amount>
<concentration units="nist:molar">5</concentration>
<substance role="solvent" ref="s324235"
title="decanes"/>
</substance>
<substance role="rsc:reagent" ref="g32423"
title="(2E)-oct-2-en-1-ol">
<amount units="nist:g">12.8</amount>
</substance>
<substance role="rsc:solvent" ref="s324234"
title="DCM">
<amount units="nist:ml">200</amount>
</substance>
</reaction>